Contract Analyses

The LabSPA – Laboratory for Scientific Particle Analysis – offers you a wide range of contract analyses for the characterization of dispersions, powders and porous materials. These can be requested as individual analyses, as call-off orders for a large number of samples in a defined period of time or as a comprehensive laboratory project. We will gladly submit you an offer. Individual sample preparation and/or measurement routines can be coordinated with our excellently trained laboratory staff.

Order-No. Parameter/ method Description
140056 Particle size distribution / Laser diffraction method (static light scattering) – wet measurement in water Determination of particle size distribution according to ISO 13320-1 in water, measuring range 0.01 – 3500 µm, the specific experimental conditions (tap water or deionized water, ultra sound treatment, dispersion additives) are chosen after consultation
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140057 Particle size distribution / Laser diffraction method (static light scattering) – dry measurement in pressurized air Determination of particle size distribution according to ISO 13320-1 by means of dry dispersion with pressurized air, measuring range 0.1 – 2600 µm
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140058 Particle size distribution / Laser diffraction method (static light scattering) – wet measurement in isopropanol Determination of particle size distribution according to ISO 13320-1 in isopropanol, 0.01 – 3500 µm
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140059 Particle size distribution / Laser diffraction method (static light scattering) – other dispersion media Determination of particle size distribution according to ISO 13320-1 in alternative liquids in consultation, measuring range 0.01 – 3500 µm
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140258 Particle size analyses / Method development laser diffraction resp. static light scattering – wet or dry measurement Optimized application of the laser diffraction to investigate the most suitable dispersion and measurement parameters for a certain material
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140060 Particle size distribution/ Combined method laser diffraction and dynamic image analysis – wet measurement Determination of particle size distribution in liquids, measurement range 0.01 – 3500 µm, beneficial especially for broad size distributions up to the mm range, the specific experimental conditions (dispersion medium, ultra sound treatment, dispersion additives) are chosen after consultation, incl. exemplary images
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140259 Particle size distribution / dynamic image analysis – dry Determination of particle size and shape analysis acc. to ISO 13322 dry; dispersing with vibratory feeder and free drop chute, measuring range 30 µm – 10 mm
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90006 Particle size distribution / Acoustic spectroscopy – wet measurement, > 5 nm Determination of particle size distribution by means of ISO 20998-1 in liquid medium, measurement in original sample concentration up to 50 Vol.-%, measurement range 5 nm – 1000 µm
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140135 Particle size distribution / Dynamic light scattering (DLS resp. PCS), in liquid medium Particle size distribution according to ISO 22412 (dynamic light scattering, DLS resp. photon correlation spectroscopy, PCS), in liquid medium, measuring range 1 nm – 9.5 µm
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140097 Particle size by sieve analysis – dry Sieving of powders, details after consultation
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140061 Particle size distribution and shape analysis/ Image analysis or/and laser – wet or dry measurement Comprehensive particle size and shape analysis, determination in liquid or dry, maximum measurement range for particle size 0.01 – 10000 µm, 4 – 10000 µm for particle shape
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Order-No. Parameter/ method Description
90007 Zeta potential / Electro acoustic Determination of the zeta potential of dispersions acc. to ISO 13099-3 in polar liquids, measuring of dispersions in original concentration up to ca. 50 Vol.-%
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90008 Zeta potential as function of the pH-value (titration)/ Electro acoustic Determination of the zeta potential of dispersions acc. to ISO 13099-3 as function of the pH-value or of additives in polar liquids, evaluation of the isoelectric point, measuring of dispersions in original concentration up to ca. 50 Vol.-%
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90009 Dielectrical permittivity Determination of the dielectric constant as measure of the permittivity of a dispersion or homogenous liquid to an electrical field
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97239 Electrical conductivity of liquid systems Determination of the electrical conductivity of non-polar and polar liquids and dispersions, 1011 – 10-4 S/m
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Order-No. Parameter/ method Description
97968 Dynamic viscosity of liquids and dispersions, one-point measurement Determination of the dynamic viscosity (mPa*s) at a specific shear rate; measured at one arbitrary temperature (4 to 80 °C) and shear rate (10 to 150000 s-1)
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97894 Dynamic viscosity of liquids and dispersions, in dependence of the shear rate Determination of the dynamic viscosity (mPa*s) in dependence of the shear rate (5 measuring points); measured at one arbitrary temperature (4 to 80 °C)
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97969 Dynamic viscosity of liquids and dispersions, in dependence of the shear rate and the temperature Determination of the dynamic viscosity (mPa*s) in dependence of the shear rate and the temperature (4 to 80 °C); measurement of five-point-viscosity curves at 5 different arbitrary temperatures
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Order-No. Parameter/ method Description
90013 Drying behavior – short time characterization/ Microrheology Analysis of the drying behavior of coatings, films or foams by adaptive speckle imaging interferometry (A.S.I.I.)
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Order-No. Parameters Description
97878 Melting behavior / Microrheology Thermal analysis of foods (e. g. chocolate, butter, etc.) and cosmetic products (fatty creams, etc.); temperature range 4 – 90 °C
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Order-No. Parameter Description
90010 Stability/ Multiple light scattering Stability analysis of emulsions and suspensions acc. to ISO TR 13097, temperature range 4 – 80° C
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90012 Heavy fuel characterization/ multiple light scattering Stability analysis of heavy fuels (Heavy Fuel Characterization acc. to ASTM D7061)
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Order-No. Parameter Description
97732 Formulation of dispersions Formulation/Deflocculation, Creation of a work instruction to stabilize or disperse a dispersion, optimization of additives and solids contents, optimization of the dispersing conditions (deflocculation method like ultrasonic treatment, stirring etc.)
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97734 Nano-material test regarding EU definition Nano-material test regarding EU definition 1/696/EU using the LabSPA-Nano-method
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97735 Dispersion project, individual We act as your project partner for your special task regarding dispersions
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Order-No. Parameter Description
140016 Angles of repose and collapse of powders Determination of angles of repose and collapse of powders according to ASTM D 6393-08/D 6393-14
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140017 Dispersibility, uniformity and cohesion of powders Determination of dispersibility, uniformity and cohesion of powders according to ASTM D 6393-08/D 6393-14
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140018 Flat plate angle (angle of spatula) of powders Determination of flat plate angle of powders according to ASTM D 6393-08/D 6393-14
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140019 Compressibility of powders Determination on Powder analyzer acc. to
ASTM D 6393-08/ D 6393-14 resp. ISO 3953:1993
Includes tap- and bulk density
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140020 Voidage of powders Determination of voidage of powders according to ASTM D 6393-08/D 6393-14
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140021 Flowability and floodability indices of powders Determination of flowability and floodability indices of powders according to ASTM D 6393-08/D 6393-14
Includes angles of repose, angle of collapse, dispersibility, uniformity, cohesion, flat plate angle, voidage, flowability and floatability indices of powders
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Order-No. Parameter Description
170158 Multipoint-BET with nitrogen Specific surface multipoint-BET-analysis by nitrogen adsorption at 77 K, acc. to ISO 9277 (volumetric method), standard is 5-point-measurement (alternative on demand), requires at least 1 m² absolute sample surface area in the sample cell
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110906 Multipoint-BET with argon Specific surface multipoint-BET-analysis by argon at 87 K, acc. to ISO 9277 (volumetric method), standard is 5-point-measurement (alternative on demand), requires at least 1 m² absolute sample surface area in the sample cell
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170159 Multipoint-BET with carbon dioxide, 273 K Specific surface multipoint-BET-analysis by carbon dioxide adsorption at 273 K, acc. to ISO 9277 (volumetric method), standard is 5-point-measurement (alternative on demand), requires at least 10 m² absolute sample surface area in the sample cell
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110907 Multipoint-BET with carbon dioxide, 195 K Specific surface multipoint-BET-analysis by carbon dioxide adsorption at 195 K, acc. to ISO 9277 (volumetric method), standard is 5-point-measurement (alternative on demand), requires at least 10 m² absolute sample surface area in the sample cell
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170160 1-point-BET with nitrogen Specific surface via 1-point-BET-analysis (p/p0 = 0.3) with nitrogen adsorption at 77 K, acc. to ISO 9277, requires min. 0.3 m² absolute sample surface area in the sample cell
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110908 Multipoint-BET with krypton (for small surfaces) Specific surface multipoint-BET-analysis with krypton adsorption at 77 K, acc. to ISO 9277 (volumetric method), standard is 5-point-measurement (alternative on demand), recommended method for absolute sample surface areas smaller than 1 m² in the sample cell
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170162 STSA surface area for the characterization of carbon blacks STSA surface area as specifically determined external surface of carbon black samples acc. to ASTM D 6556 (volumetric method), with additional determination of the BET surface area
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170163 Micropore surface / Micropore volume Micropore surface area and volume with nitrogen adsorption at 77 K, evaluation acc. to t-method or Dubinin-Radushkevic acc. to DIN 66135-3 (volumetric method) and BET surface area (ISO 9277)
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Order-No. Parameter Description
90015 Pore size distribution/Pore volume Hg-intrusion and extrusion: Measurement range ca. 1000 µm − 0,0036 µm pore diameter, pore volume and pore size distribution acc. to ISO 15901-1
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90020 Extended porosimetry Hg-intrusion and extrusion: Measurement range ca. 1000 µm − 0,0036 µm pore diameter, pore volume and pore size distribution acc. to ISO 15901-1, additional determination of density, raw density and porosity [%] (from the raw density of the Hg-porosimetry and density of the He-pycnometry)
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97436 Hg contact angle measurement Measurement of the sample´s mercury contact angle by determination of the intrusion pressure of a capillary with known diameter
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Order-No. Parameter Description
170164 BET-surface area, pore volume, average pore size, N2 Determination by nitrogen adsorption at 77 K (alternative on demand)
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110909 BET-surface area, pore volume, average pore size, Ar Determination by argon adsorption at 87 K (alternative on demand)
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170165 Standard mesopore analysis (BJH-method), N2 77 K Determination by nitrogen adsorption at 77 K, 20 points adsorption plus 35 points desorption, max. detectable pore diameter ca. 0.4 µm (limited by the method of gas sorption), BJH-pore size distribution (DIN 66134), alternative DFT-evaluation, pore volume, BET-surface area (ISO 9277)
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110910 Standard mesopore analysis (BJH-method), Ar 87 K Determination by argon adsorption at 87 K, 20 points adsorption plus 35 points desorption, max. detectable pore diameter ca. 0.4 µm (limited by the method of gas sorption), BJH-pore size distribution (DIN 66134), alternative DFT-evaluation, pore volume, BET-surface area (ISO 9277)
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170166 High resolution mesopore analysis, N2 77 K Determination by nitrogen adsorption at 77 K, 40 points adsorption plus 39 points desorption, max. detectable pore diameter ca. 0.4 µm (limited by the method of gas sorption), BJH-pore size distribution (DIN 66134), alternative DFT-evaluation, pore volume, multipoint-BET-surface area (ISO 9277)
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110911 High resolution mesopore analysis, Ar 87 K Determination by argon adsorption at 87 K, 40 points adsorption plus 39 points desorption, max. detectable pore diameter ca. 0.4 µm (limited by the method of gas sorption), BJH-pore size distribution (DIN 66134), alternative DFT-evaluation, pore volume, multipoint-BET-surface area (ISO 9277)
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170167 Micropore analysis Determination by nitrogen adsorption at 77 K or carbon dioxide at 273 K, BET (ISO 9277) and pore volume, depending on sample material and customer requirement the most suitable micropore evaluation is applied (DR, DA, HK, SF, DFT, GCMC), (DIN 66135, part 1 to 4)
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110912 Micropore analysis Determination by argon at 87 K or carbon dioxide at 195 K, BET (ISO 9277) and pore volume, depending on sample material and customer requirement the most suitable micropore evaluation is applied (DR, DA, HK, SF, DFT, GCMC), (DIN 66135, part 1 to 4)
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110913 Micropore analysis of pore systems < 0.7 nm (molecular probe method) Determination of the real micropore distribution and sorption behavior of microporous materials by several adsorptives with different critical molecule diameters of ca. 0.26 – 0.7 nm
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170168 Micropore and mesopore analysis, N2 Determination by nitrogen sorption at 77 K, ca. 70 points adsorption plus ca. 20 points desorption, BET (ISO 9277), pore volume and mesopore distribution (DIN 66134), depending on sample material and customer requirement the most suitable micropore evaluation is applied (DR, DA, HK, SF, DFT, GCMC), (DIN 66135, part 1 to 4)
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110914 Micropore and mesopore analysis, Ar Determination by argon adsorption at 87 K, ca. 70 points adsorption plus ca. 20 points desorption, BET (ISO 9277), pore volume and mesopore distribution (DIN 66134), depending on sample material and customer requirement the most suitable micropore evaluation is applied (DR, DA, HK, SF, DFT, GCMC), (DIN 66135, part 1 to 4)
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110916 Micropore analysis of carbon materials Determination by carbon dioxide adsorption (ca. 40 points adsorption) at 273 K, pore size distribution, pore volume and specific surface area by NLDFT or Monte-Carlo-Simulation; from 0.35 nm to 1.5 nm
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110917 sotherm measurement in the normal pressure range Isotherm measurement in the normal pressure range, e.g. H2, CH4, CO2, n-butane, CO, SF6, i-butane; sorption analysis of non-corrosive gases as adsorption and desorption isotherm at temperatures from 20 to 323 K
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110918 Determination of adsorption enthalpy in normal- and high pressure range up to 200 bar Determination of isosteric adsorption heats from three isotherms at different temperatures as function of the amount adsorbed
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97499 High pressure adsorption isotherm up to 200 bar, from 77 K up to 400 °C High pressure adsorption isotherm (non-corrosive gases), e.g. H2, CO2, CH4, CO; sorption analysis of non-corrosive gases as adsorption and desorption isotherm up to 200 bar, temperature from 77 K to 673 K
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90030 Evaluation of gas sorption analyses (from external data) acc. to state-of-the-art evaluation methods Evaluation of gas sorption analyses (out of external data) acc. to state-of-the-art evaluation methods. Calculation of pore size distributions out of external data (ASCII-files). Includes data import into the evaluation software, evaluation acc. to Density Functional Theory (DFT) and / or Monte-Carlo-Simulation (GCMC)
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Order-No. Parameter Description
215164 Characterization of through-pore-systems, standard Pore size distribution of through-pores of materials like filters, membranes, woven and non-woven, ca. 13 nm to 500 µm
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215165 Characterization of through-pore-systems, special Pore size distribution of through-pores of materials like filters, woven and non-woven, membranes, frits, ca. 2 nm to 500 µm with special sample preparation or liquid-liquid-porometry
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215166 Gas permeability up to 35 bar Determination of the gas permeability of filters, membranes and other solids at constant or variable pressures
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215167 Liquid permeability up to 35 bar Determination of the liquid permeability of filters, membranes and other solids at constant or variable pressures
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Order-No. Parameter Description
170173 Density (true density) of solids by gas pycnometry Determination by helium pycnometry at 25 °C acc. to DIN 66137-2, other temperatures and alternative gases on request
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97500 Density (true density) of solids Density measurement of solids by Archimedes’ principle (buoyancy method)
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97501 Density of liquids Density measurement of homogeneous liquids by Archimedes’ principle (buoyancy method)
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97502 Density of dispersions Density measurement of dispersions (suspensions resp. emulsions) acc. to the pycnometer principle
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140260 Tap density Determination by defined compaction acc. to ISO 787/11: Sample volume (density) is evaluated every 500 tap cycles and the compaction is continued until the constant volume is reached
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140261 Bulk density For powders and granulates in the measuring cylinder
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90090 Raw density Gravimetric determination by mercury pycnometry at ambient pressure
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97503 Raw density Raw density measurement by Archimedes’ principle (buoyancy method)
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140262 Raw density Raw density measurement by envelopping with pycnometric powder
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Order-No. Parameter Description
170174 Closed cell determination, uncorrected Determination of the open and closed cell content in rigid foams, DIN EN ISO 4590 − uncorrected (without cross section pores)
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170175 Closed cell determination, corrected Determination of the volume share of open and closed cells in rigid foams, DIN EN ISO 4590 − corrected (cross section pores considered)
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170176 Foam material characterisation, compressibility Determination of the compressibility of soft foams in the pressure range 2 – 20 PSI (0.13 − 1.3 bar)
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170177 Vacuole volume of milk powder Determination of the vacuole volume of milk powder by nitrogen pycnometry
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Order-No. Parameter Description
97274 Water vapor isotherm, adsorption and desorption, gravimetric Gravimetric determination of water vapor isotherm, humidity ca. 2 – 96 %, analysis temperature 10 – 80 °C, adsorption and desorption
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97390 Water vapor isotherm adsorption, desorption and sorption kinetics, gravimetric Gravimetric determination of the water vapor isotherm, humidity ca. 2 – 96 %, analysis temperature 10 – 80 °C, adsorption , desorption and kinetics
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90081 Water vapor isotherm, adsorption and desorption, static-volumetric Determination of the water vapor sorption up to ca. 96 %, 10 different humidities, analysis temperature 12 to 85 °C, adsorption and desorption, manometric method
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90082 Water vapor isotherm, adsorption Determination of the water vapour sorption up to ca. 96 %, 10 different humidities, analysis temperature 12 to 85 °C, adsorption
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90083 High resolution water vapor isotherm, adsorption and desorption Determination of the water vapour sorption up to ca. 96 %, 40 different humidities, analysis temperature 12 – 85 °C, adsorption and desorption, manometric method
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90084 Water vapor isotherm, hysteresis behaviour Determination of the water vapor sorption up to ca. 98 %, 10 different humidities, analysis temperature 12 – 85 °C, additionally one repeated adsorption and desorption cycle, manometric method
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90085 Water vapor isotherm incl. determination of the adsorption heat Determination of the water vapor sorption up to ca. 96 % relative humidity at 10 different humidities at two different temperatures, 12 – 80 °C, adsorption and desorption, calculation of the water vapor sorption enthalpy
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170178 Vapor sorption, static-volumetric Determination of the vapor sorption (e.g. water, alcohols, pyridine), adsorption and desorption
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Order-No. Parameter Description
170179 Chemisorption analysis, volumetric method Determination of the monolayer capacity, degree of dispersion, active surface acc. to DIN 66136-1, DIN 66136-2: static-volumetric, e.g. H2, NH3, CO, CO2, O2
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315051 Chemisorption analysis, flow method (dynamic) Determination of the monolayer capacity, degree of dispersion, active surface (DIN 66136-1, DIN 66136-3: flow method), e.g. H2, NH3, CO, CO2, O2
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315052 Temperature programmed reactions (TPD/TPR/TPO a.o.) Customer specific temperature programmed reactions (desorption, reduction, oxidation a.o.), determination of the activation energy and/or desorption energy
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315053 Temperature programmed reactions (TPD/TPR/TPO a.o.) with mass spectrometer Customer specific temperature programmed reactions (desorption, reduction, oxidation a.o.), determination of the activation energy and/or desorption energy as well as analysis of reaction products by mass spectrometry
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Order-No. Parameter Description
330020 Investigation of the regenerability of adsorbents Investigation of the regenerability and cycle stability of adsorbents , adsorption and desorption cycles are repeated with regard to the stable sorption behavior of the adsorbents
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330009 Adsorption equilibrium points of gas mixtures Adsorption of gas mixtures > 2 components with appropriate analysis
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330010 IAST-calculations Calculation of mixture gas adsorption with a maximum of 4 components according to the IAST model (ideal adsorbate gas behavior)
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330011 PRAST-calculations Calculation of binary gas/vapor mixtures according to the PRAST and UNIQUAC model (real adsorbate phase behavior)
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330012 Kinetics – Diffusion From adsorption amount vs. time, with model calculation
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330013 Uptake – Kinetics From adsorption amount vs. time, without model
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Order-No. Parameter Description
330014 Breakthrough curves of pure gases and vapors on textiles On textiles
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110781 Breakthrough curves of non-corrosive gases on adsorber packed beds Measuring of breakthrough curves of gases as well as kinetic data under technically relevant conditions
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110782 Breakthrough curves of gases and vapors on packed beds Measuring of breakthrough curves of gases as well as kinetic data under technically relevant conditions
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110321 mixSorb-Messungen mixSorb-Messungen divers nach Absprache
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330017 Breakthrough curves of corrosive gases on adsorber packed beds Measuring of breakthrough curves of gases as well as kinetic data under technically relevant conditions
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330018 Uptake -Kinetics From adsorption amount vs. time, without model
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Order-No. Parameter Description
330019 Adsorption of components ouf of aqueous phase Adsorption equilibrium in liquid phase after 48 h shaking, with analysis GC resp. HPLC
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330034 Particular tests concerning adsorption of components out of aqueous phase Special tasks within the scope of liquid phase adsorption are tested and a jointly prepared SOP on the procedure is processed accordingly
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Order-No. Parameter Description
330021 Thermogravimetry pure gas 1 bar Up to max. 1600 °C in inert gas or air, pure gases p = 1 bar
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330022 Thermogravimetry gas mixtures 1 bar Up to max. 1600 °C in gas mixtures p = 1 bar
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330023 Thermogravimetry up to 5 bar Up to max. 1600 °C in inert gas, air or gas mixtures up to 5 bar
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330024 Thermogravimetriy with MS or other analytics -100 °C to max. 1600 °C in vacuum < p < 5 bar
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98052 DTA/DSC Thermoanalytical examination by means of DTA or DSC
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Order-No. Parameter Description
90116 Light microscopy Light microscopic investigations of your samples by prior arrangement
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90117 Scanning electron microscopy Scanning electron microscopic investigations of your samples by prior arrangements
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Order-No. Parameter Description
90119 Structural analysis Elucidation of the chemical composition of chemical compounds
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90120 Chemical analysis Identification and quantification of chemical substances
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330026 Elemental analysis content of C, H, N, O, S, Cl
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330027 Element specification Preparation for element determination, ash content and digestion, AAS for one element, e.g. Cr or Ni content, or ICP-OES, e.g. for total screening
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330028 Headspace-GC Vapor analysis for the determination of the concentration of volatile substances of a solution in the vapor above the solution
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Order-No. Parameter Description
330029 Thermal conductivity On beds, stationary temperature difference
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330030 Electrical resistance On a single grain, resistance referring to the weight of the stamp
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97970 Spontaneous combustion Double determination of spontaneous inflammation
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Order-No. Parameter Description
97710 Drying loss Determination of drying loss
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97695 Dry content Determination of dry content of solid in water
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330004 Sample division Representative riffling, max. 120 ml
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330005 Sample division Representative riffling, max. 2500 ml
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330006 pH-value pH-measurement
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330007 Conductivity (aqueous) Measurement of conductivity in aqueous dispersions
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98038 Specific sample preparations resp. lump-sum fee The specific sample preparation requests will be audited, the relevant sample preparation SOP will be processed resp. lump-sum fee
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Order-No. Parameter Description
90115 Method development and project work Combined application of analysis methods aimed to investigate the applicability of methods for a certain task.
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97509 Take-over of external quality control Take-over of analyses for your quality control by mutual agreement: if necessary, analyzers are reserved according the schedule, accordingly calibrated and checked previous to an analysis series.
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97511 Seminars Internal (in our laboratory) or external (at your site) seminars provide advantages for the training of groups: We offer a package price (seminar, training, travel expenses incl.) and we define topics and duration of the training (seminar) after consultation with you.
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97512 Comparison measurements with customer specific analysis conditions We analyse your samples according to your instructions for comparison with your analysis results, which you obtained either by using the same analyzer type or different ones or by alternative analysis methods, and evaluate the results.
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97513 Product expert consultation Our accordingly specialized product expert handles your task, works on the requirements and provides a written report as well as a final discussion
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97515 Analyzer rental incl. user training The analyzers of the LabSPA can be rented upon prior arrangement, we provide a quotation for the analyzer rental incl. installation and user training at your site.
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97516 Cost effective rental of the laboratory („Rent the lab“) Analyzers of the LabSPA can be rented incl. working time of the required lab staff. The invoice for analysis results is not based on the number of performed analyses but on the number of working days. This is advantageous when applying different analysis methods (parallel use of analyzers) and if you wish to be present during measurements.
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